FIGURES

Fig. 3.1: Diagram: percolation curves of carbon.black with various size specific surface areas and various size empty volumes [72a].

Fig. 3.2: SEM-picture of a carbon-black compound with a carbon- black concentration of 5% [17d].

Fig. 3.3:Schematic representation of an apparature to measure the shear rate [76].

Fig. 3.4: Viscosity curves [76].

Fig. 3.5: printout of a computer aided interpolation [76].

Fig. 3.6: Schematic representation of the pyrolization apparatures [76].

Results of measurements and corrections. Dynamic Viscosity in slope of the Volume-portion-dispersed phase [76]:

Fig. 3.7: Pebax 2533 with Printex XE-2 and wax

Fig. 3.8: Pebax 2533 with Printex XE-2

Fig. 3.9: PS N 2000 with Printex XE-2 and wax

Fig. 3.10: PS N 2000 with Printex XE-2

Fig. 3.11: Pebax 2533 with Black Pearls 880 Monarch and wax

Fig. 3.12: PS N 2000 with Black Pearls 880 Monarch and wax

Fig. 3.13: PS N 2000 with Black Pearls 880 Monarch

Fig. 3.14: PS N 2000 with titanium dioxide RL 90

Results of measurements and corrections : Dynamic Viscosity in slope of the Volume Portion Filler [76]:

Fig. 3.15:

Fig. 3.16:

Fig. 3.17:

Fig. 3.18:

Fig. 3.19:

Results of measurements and corrections: pyrolytic measurements [76]:

Fig. 3.20: PS N 2000 with carbon black

Fig. 3.21: PS N 2000 with titanium dioxide RL 90

Fig. 3.22: Pebax 2533 with carbon black

Fig. 3.23: Carbon black concentrates with Printex XE-2. Conductivity vs. Carbon-Black Portion [76].

Dynamic viscosity compared to the volume portion dispersed phase [76]:

Fig. 3.24: PS N 2000 with Printex XE-2

Fig. 3.25: PS N 2000 with Printex XE-2, modified scale

Fig. 3.26: Pebax 2533 with Printex XE-2 and wax


Footnotes

[1] The conductivity curves of a number of samples are shown in a figure in sub-section 3.3.3.2

[2] See footnote 3 on page 7.

[3] 80% is the result of the following calculation: pyrolysis residue minus the carbon black concentration in the compound gives the quantity which is then calculated as a percentage of the carbon black content. Thus if a 1% (mass%) carbon black compound has a residue of 1.8%, this means an 80% excess.

[4] Identifiable by "melt fracture" (roughened, often fish-scale-like surface)

[5] Weighing precision 1/10 g

[6] Term describing the layer of plastic that wraps around the roller.

[7] It was only possible to analyse one series of measurements, as the wax migrated to the surface, thereby distorting the viscosities in the subsequent measurements. Cf. sub-section 3.4.



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