FIGURES
Fig. 3.1: Diagram: percolation curves of carbon.black with various size specific surface areas and various size empty volumes [72a].
Fig. 3.2: SEM-picture of a carbon-black compound with a carbon- black concentration of 5% [17d].
Fig. 3.3:Schematic representation of an apparature to measure the shear rate [76].
Fig. 3.4: Viscosity curves [76].
Fig. 3.5: printout of a computer aided interpolation [76].
Fig. 3.6: Schematic representation of the pyrolization apparatures [76].
Results of measurements and corrections. Dynamic Viscosity in slope of the Volume-portion-dispersed phase [76]:
Fig. 3.7: Pebax 2533 with Printex XE-2 and wax
Fig. 3.8: Pebax 2533 with Printex XE-2
Fig. 3.9: PS N 2000 with Printex XE-2 and wax
Fig. 3.10: PS N 2000 with Printex XE-2
Fig. 3.11: Pebax 2533 with Black Pearls 880 Monarch and wax
Fig. 3.12: PS N 2000 with Black Pearls 880 Monarch and wax
Fig. 3.13: PS N 2000 with Black Pearls 880 Monarch
Fig. 3.14: PS N 2000 with titanium dioxide RL 90
Results of measurements and corrections : Dynamic Viscosity in slope of the Volume Portion Filler [76]:
Results of measurements and corrections: pyrolytic measurements [76]:
Fig. 3.20: PS N 2000 with carbon black
Fig. 3.21: PS N 2000 with titanium dioxide RL 90
Fig. 3.22: Pebax 2533 with carbon black
Fig. 3.23: Carbon black concentrates with Printex XE-2. Conductivity vs. Carbon-Black Portion [76].
Dynamic viscosity compared to the volume portion dispersed phase [76]:
Fig. 3.24: PS N 2000 with Printex XE-2
Fig. 3.25: PS N 2000 with Printex XE-2, modified scale
Fig. 3.26: Pebax 2533 with Printex XE-2 and wax
[1] The conductivity curves of a number of samples are shown in a figure in sub-section 3.3.3.2
[2] See footnote 3 on page 7.
[3] 80% is the result of the following calculation: pyrolysis residue minus the carbon black concentration in the compound gives the quantity which is then calculated as a percentage of the carbon black content. Thus if a 1% (mass%) carbon black compound has a residue of 1.8%, this means an 80% excess.
[4] Identifiable by "melt fracture" (roughened, often fish-scale-like surface)
[5] Weighing precision 1/10 g
[6] Term describing the layer of plastic that wraps around the roller.
[7] It was only possible to analyse one series of measurements, as the wax migrated to the surface, thereby distorting the viscosities in the subsequent measurements. Cf. sub-section 3.4.